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Extra resources for Amino Acids, Peptides and Proteins (SPR Amino Acids, Peptides, and Proteins (RSC))vol.16

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1983, 24, 3427. 10 Amino Acids, Peptides, and Proteins CONH, I I PhCH,OCH + ii 0x0 Me Me + O V CH-OH H OMexMe0 Reagents: i, known sequence; ii, modified Strecker-type synthesis; iii, hydrolysis, CSCh; iv, Corey-Winter reaction Scheme 3 and allylic substitution through alkylation of the n-allylpalladium complex with carbanions from t-butyl acetoacetate or MeCOCH2SPh) have been described. loo Synthesis of 0- and Higher Homologous Natural Amino Acids. 1°4 a-Alkyl Analogues of Natural a-Amino Acids.

Ozer, and A. Ulzegha, Rend. Semin. Fac. Sci. Univ. Cagliari, 1982, 52, 159 (Chem. , 1983, 99, 1 7 4 8 6 0 ) . 294 J. M. Aizpurua and C. Palomo, Synth. , 1983, 13, 745. 29 5 S . Kim and H . Chang, J. Chem. ,Chem. , 1983, 1357. 2 96 G . Perseo, S. Piani, and R . De Castiglione, Int. J. Pept. Protein R e s . , 1983, 21, 227. 291 A . K. Rabinovich, V . N. Karelskii, E. P. Krysin, A. A. Antonov, M. B. Smirnov, and G. Cipens, Khim. Prir. , 1983, 216. 298 C . R. McArthur, P. M. Worster, and A. U. Okon, Synth.

Vasella, R. Voeffray, J. Pless, and R. Huguenin, Helv. Chim. Acta, 1983, 66, 1241. 113 R. Henning and H. Urbach, Tetrahedron L e t t . , 1983, 24, 5339. lo5 Io6 13 Amino Acids 0 aH i NHAc \ H H 1 iii, iv H Reagents: i, MeCN, Hg(NO,),, NaCl; ii, CH,=C(CN)Cl, NaBH,; iii, NaH-DMF; iv, refluxing 5M HC1 Scheme 6 have described a stereospecific synthesis of 4,s -disubstituted proline analogues starting from an alkene (Scheme 6),'14 verifying the stereochemistry through X-ray crystal a n a 1 y ~ i s .

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